Alpha-Fe2O3 Synthesis by Sol-Gel Technique and Characterization [LAB MANUAL]

This semester, in the Nanoscience Lab, I was required to prepare alpha-Fe2O3(Hematite) by sol-gel method for my first experiment. This was a great experience as I learned a lot of new stuff and got to use cool instruments during the labs. Using my knowledge, and whatever I learnt, I have tried to create a detailed lab manual for the experiment for future students.

Alpha-Fe2O3 (Cell)


To prepare alpha-Fe2O3 nanoparticles by sol-gel technique and study the effect of different annealing temperatures and heating times on the crystallite size using the peak widths of the diffractograms(XRD) of the differently prepared

Version 2

Here I am attaching a PDF version of the Lab Manual that I created. This is the version 2.0.
It contains observations about all the 4 samples. However, there are still some things that I need to add like the interplanar spacings and lattice parameter calculations and some info in the Results and Discussion section.
Download: PDFfe2o3 xrd compressed ver 2

Version 1

Currently, the manual contains info about 2 samples, but it will be updated soon.
Here I am attaching a PDF version of the Lab Manual that I created. This is the version 1.0.
It contains information about 2 samples.
fe2o3 xrd

PhD researcher at Friedrich-Schiller University Jena, Germany. I'm a physicist specializing in computational material science. I write efficient codes for simulating light-matter interactions at atomic scales. I like to develop Physics, DFT and Machine Learning related apps and softwares from time to time. Can code in most of the popular languages. Like to share my knowledge in Physics and applications using this Blog and a YouTube channel.
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